Characterisation of nanocrystalline PZT synthesised via a hydrothermal method

S. Harada; S. Dunn

Characterisation of nanocrystalline PZT synthesised via a hydrothermal method

S. Harada, S. Dunn

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

Abstract

This paper describes the progress made toward characterising lead zirconate titanate (PZT) synthesised via a novel hydrothermal method [1,2]. Low temperatures (≤ 200°C) and high mineraliser (potassium hydroxide) concentrations were used to produce single-phase, perovskite PZT in a bomb-type reactor. Full phase purity was attained after just 30 minutes of processing at 160°C. The particles had a wide size distribution, from nanoscale agglomerates with irregular morphology, up to micronsized cubes. It is believed that the differences in morphology can be attributed to two distinct formation stages.

Original language	English
Title of host publication	2005 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2005 Technical Proceedings
Editors	M. Laudon, B. Romanowicz
Pages	17-20
Number of pages	4
Publication status	Published - 12 May 2005
Externally published	Yes
Event	2005 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2005 - Anaheim, CA, United States Duration: 8 May 2005 → 12 May 2005

Publication series

Name	2005 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2005 Technical Proceedings

Conference

Conference	2005 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2005
Country/Territory	United States
City	Anaheim, CA
Period	8/05/05 → 12/05/05

Keywords

Hydrothermal
Nanocrystalline
PZT

Cite this

@inproceedings{2aeb50a8d48d4232b2f8661890b885fe,

title = "Characterisation of nanocrystalline PZT synthesised via a hydrothermal method",

abstract = "This paper describes the progress made toward characterising lead zirconate titanate (PZT) synthesised via a novel hydrothermal method [1,2]. Low temperatures (≤ 200°C) and high mineraliser (potassium hydroxide) concentrations were used to produce single-phase, perovskite PZT in a bomb-type reactor. Full phase purity was attained after just 30 minutes of processing at 160°C. The particles had a wide size distribution, from nanoscale agglomerates with irregular morphology, up to micronsized cubes. It is believed that the differences in morphology can be attributed to two distinct formation stages.",

keywords = "Hydrothermal, Nanocrystalline, PZT",

author = "S. Harada and S. Dunn",

year = "2005",

month = may,

day = "12",

language = "English",

isbn = "0976798514",

series = "2005 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2005 Technical Proceedings",

pages = "17--20",

editor = "M. Laudon and B. Romanowicz",

booktitle = "2005 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2005 Technical Proceedings",

note = "2005 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2005 ; Conference date: 08-05-2005 Through 12-05-2005",

}

Harada, S & Dunn, S 2005, Characterisation of nanocrystalline PZT synthesised via a hydrothermal method. in M Laudon & B Romanowicz (eds), 2005 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2005 Technical Proceedings. 2005 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2005 Technical Proceedings, pp. 17-20, 2005 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2005, Anaheim, CA, United States, 8/05/05.

Characterisation of nanocrystalline PZT synthesised via a hydrothermal method. / Harada, S.; Dunn, S.
2005 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2005 Technical Proceedings. ed. / M. Laudon; B. Romanowicz. 2005. p. 17-20 (2005 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2005 Technical Proceedings).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

TY - GEN

T1 - Characterisation of nanocrystalline PZT synthesised via a hydrothermal method

AU - Harada, S.

AU - Dunn, S.

PY - 2005/5/12

Y1 - 2005/5/12

N2 - This paper describes the progress made toward characterising lead zirconate titanate (PZT) synthesised via a novel hydrothermal method [1,2]. Low temperatures (≤ 200°C) and high mineraliser (potassium hydroxide) concentrations were used to produce single-phase, perovskite PZT in a bomb-type reactor. Full phase purity was attained after just 30 minutes of processing at 160°C. The particles had a wide size distribution, from nanoscale agglomerates with irregular morphology, up to micronsized cubes. It is believed that the differences in morphology can be attributed to two distinct formation stages.

AB - This paper describes the progress made toward characterising lead zirconate titanate (PZT) synthesised via a novel hydrothermal method [1,2]. Low temperatures (≤ 200°C) and high mineraliser (potassium hydroxide) concentrations were used to produce single-phase, perovskite PZT in a bomb-type reactor. Full phase purity was attained after just 30 minutes of processing at 160°C. The particles had a wide size distribution, from nanoscale agglomerates with irregular morphology, up to micronsized cubes. It is believed that the differences in morphology can be attributed to two distinct formation stages.

KW - Hydrothermal

KW - Nanocrystalline

KW - PZT

UR - https://www.scopus.com/pages/publications/32144456592

M3 - Conference contribution

AN - SCOPUS:32144456592

SN - 0976798514

SN - 9780976798514

T3 - 2005 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2005 Technical Proceedings

SP - 17

EP - 20

BT - 2005 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2005 Technical Proceedings

A2 - Laudon, M.

A2 - Romanowicz, B.

T2 - 2005 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2005

Y2 - 8 May 2005 through 12 May 2005

ER -

Characterisation of nanocrystalline PZT synthesised via a hydrothermal method

Abstract

Publication series

Conference

Keywords

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Cite this